PTFE Electroless Nickel Instructions

PTFE Electroless Nickel Instructions

                                                                            7696 Route 31
                                                                            Lyons NY 14489
                                                                            Voice: 315.946.1213 Fax: 315.946.4456
                                                                            www.caswellplating.com


                                              PTFE ELECTROLESS NICKEL


PTFE or Teflon is an excellent coating for providing low friction values on parts, especially where two parts are sliding together. It is
especially useful on tools, molds, dies, cylinders, gun parts, bearings etc. and provides self lubricating properties to the parts it is
applied to.

Our PTFE Electroless Nickel plates a mid-phosphorous nickel plating, with 20-25% PTFE deposits.

The coating is applied in approx 1 hour to steel, copper, brass, bronze, zincated aluminum. Other metals can be plated with other
processes first, such as Flash Copper, then plated with PTFE EN.

The EN PTFE system plates at approx 0.2-0.4 mils per hour (0.0002” – 0.0004”).

Bath Prep:

Per 1.5 Gal total bath size:

    1.   Add 8 fl oz Part A
    2.   Add 28 fl oz Part B
    3.   Add 156 fl oz Distilled Water
    4.   Add 1 oz (28gm) (by weight) PTFE Dispersion
    5.   Add all the fume balls (these help keep heat in the tank)
    6.   Mark the liquid level with a permanent marker on the outside of the tank.
    7.   Mix solution with plastic spoon.
    8.   Refer to the next page for nickel credit calculations and write down your starting credit number on the balance sheet.

Bath Operation:

    1.   Calculate the surface area of the part in square inches and the time you plan to plate the part.
    2.   Consider the amount of nickel credits you will be using (# of minutes x surface area in sq inches). For example, if your part is
         10 sq inches, and you want to plate for 30 mins, you will use 300 credits (10 x 30)
    3.   Mix up the required amount of Part A and Part C to replenish all the credits you will use. Refer to next page for instructions.
    4.   Heat the bath to 190 deg F on a range or hot plate. Monitor the temperature with the included thermometer.
    5.   Hang your cleaned and waterbreak tested part from a piece of string or wire and immerse in the tank.
    6.   Plate until desired thickness is reached. Every 10 minutes or so, add a portion of your replenishment mix, and top off with
         distilled water to the original marked level.
    7.   While plating, use the part, or a plastic spoon, to keep the solution stirred up. This prevents the PTFE particles from settling
         to the bottom of the tank. Note: Pump agitation or air agitation is not recommended, as this is too vigorous and damages the
         PTFE particles.

Replenish Bath:

    1.   After plating is completed, replenish the bath with your remaining replenisher and top off to original level with distilled
         water.
    2.   Refer to the next page for replenishment procedures.
     PROCEDURE                         SETUP                         OPERATING                    EQUIPMENT                SAFETY
                                                                    PARAMETERS
      1. SURFACE            Buff & Polish for a mirror finish. Bead Blast for a ‘flat’ finish. Nylon Abrasive wheel buff for a ‘scratched
     PREPARATION            brush’ look.
                                                              140- 200 deg F                    1 x 5 gal tank       Wear rubber gloves
                                                              No agitation                      1 x tank lid         and goggles. Do not
                                                              5 mins immersion                  1 x lid ring         ingest
    2. DEGREASING                                                                               1 x 200f heater
                                                              12 oz SP Degreaser                1 x 2lb SP
                                                              3 gal Distilled water             Degreaser



  RINSE IN DISTILLED
    WATER SPRAY




 WATER BREAK TEST
                            Oil/dirt film makes water bead up        No oil/dirt film allows water to cover part
                            Aluminum: Zincate part, rinse, then immediately plate with Regular Electroless Nickel first. Do not allow to
  OPTIONAL SURFACE
                            dry between plates.
    PREPARATION
                            Steel, Iron: where corrosion may be a problem, plate for 20 mins in Regular Electroless Ni.



  RINSE IN DISTILLED
    WATER SPRAY

CALCULATE TOTAL SURFACE AREA AND PLATING TIME
CALCULATE CREDITS
CHECK for MAXIMUM LOAD 1.5 Gal plating solution = 150 sq inches of plating surface area MAXIMUM!
PREMIX REPLENISHER IF NEEDED
                                                 190 deg F                              1 x Glass Lined             Wear rubber gloves
                                                 1.5 gal setup =                        Tank                        and goggles. Do not
                                                 8 oz A, 28 oz B,                       1 x thermometer             ingest
                                                 156 oz Distilled water                 1 x Fume Balls
    3. Tank Makeup                               1 oz by weight PTFE Dispersion

                                                        pH = 6.1-6.5
                                                        MARK TANK WITH LIQUID LEVEL
                                                        NOW
4. Plating Times              Time    60 mins.         Plate Thickness       0.0002 “ – 0.0004”
  Tank Size      MAXIMUM           Square inches
                                              REPLENISH                           REPLENISHER
    In pints        LOAD             available  AFTER         Amounts required to make up enough to replenish TOTAL
                 in sq inches                PLATING SQ                      amount of credits in tank
                                               INCHES
                                                             Part A        Part C          PTFE Dispersion
      12            150          1100            220         1.5 fl oz     3 fl oz         5gm or 0.15 oz by weight
      24            300          2200            440         3 fl oz       6 fl oz         10 gm or 0.3 oz by weight
      36            450          3300            660         4.5fl oz      9 fl oz         15 gm or 0.45 oz by weight
5. DETERMINE WHEN TO REPLENISH and HOW FREQUENTLY & check temperature
After replenishing:
6. TOP UP TANK TO ORIGINAL LEVEL WITH DISTILLED WATER.
MAXIMUM LOAD
You may ONLY plate a maximum of 150 sq inches of surface area per 1.5 Gal of plating solution

If this amount is exceeded the bath will start to overwork and plating quality will seriously deteriorate.
Therefore if the part is 300 square inches, you need a MINIMUM 3 Gal Of plating solution.
Of course, if your bath contains MORE solution, this is OK.


NICKEL REPLENISHMENT
In practice, the additions of ‘replenishment’ should be made during the actual plating process at approximately every 10 minutes. The
total amount of replenishment should be calculated and made up beforehand. Ideally, the bath should be maintained at 80%
efficiency. Letting the nickel deplete below 70% level will accelerate deterioration of the bath.
Failure to replenish the solution will result in the bath eventually becoming out of balance and unusable.

The Nickel Bath Replenishment is a straightforward matter of adding more nickel from the Concentrate Part A, with an addition of
Concentrate Part C and more PTFE dispersion.

A note on bath replenishment.

During the process of plating, a quantity of water will evaporate from the tank. Additions of DISTILLED WATER must be added
periodically to maintain the correct dilution of the solution.

Make a note of the waterline when you first make up your solution. To make an addition, first, IF REQUIRED, add a quantity of
REPLENISHMENT SOLUTION, and then top up with distilled water.
It is always advisable to add small amounts of both distilled water and replenisher frequently, say every 5 minutes, as this will keep
the bath from cooling and becoming unstable.

Keep a note of the temperature when adding Replenishment. The solution should ideally be at 190 deg F when adding to ensure the
temperature drop does not go below 185 deg F.


Operating the Kit

Areas not requiring to be plated may be masked with 2 coats of Mask-it. This should be allowed to thoroughly dry between coats,
otherwise the hot solution may cause the coating to peel.

Important. Any part that contains copper, brass or bronze must be pre-plated with nickel.